K. C. Engineers Limited
K. C. Engineers Limited
Ambala, Haryana
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Chemical Reaction Engineering Lab

We are a leading Manufacturer of continuous stirred tank reactor (compressed air feed system), continuous stirred tank reactor (peristaltic pump feed system), continuous stirred tank reactor (constant head feed system), isothermal continuous stirred tank reactor, cascade continuous stirred tank reactor and r.t.d. studies in continuous stirred tank reactor from Ambala, India.
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Continuous Stirred Tank Reactor (Compressed Air Feed System)

Continuous Stirred Tank Reactor (Compressed Air Feed System)
 
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Product Details:
Model Name/NumberKCCRE-101A
ReactorMaterial Stainless Steel,Capacity 2 Ltrs (Approx)
StirrerStainless Steel Impeller and shaft coupled with FHP Motor
Feed TankMaterial Stainless Steel,Capacity - 20 Ltrs. (Approx).
Feed CirculationBy compressed air
Flow MeasurementRotameter 2Nos. (one each for Reactants).

In an ideal CSTR (i.e. an ideal steady state flow reactor)the contents in reactor are well mixed and have uniformcomposition throughout. Thus the exit stream has thesame composition as the fluid within the reactor. Thistype of reactor is known as mixed flow reactor. This setupis used to study a non-catalytic homogeneous secondorder liquid phase reaction under ambient condition.The set up consists of two feed tanks through which tworeactants are fed to the reactor. Rotameters are providedto measure the individual flow of Chemicals. The flowrate can be adjusted by operating the needle valvesprovided on respective Rotameter. The compressed air isused for circulation of feed. The CSTR is fitted with stirrerfor proper mixing. From top outlet of it samples arecollected for analysis. Pressure Regulator, Pressure Gaugeand Safety Valve are fitted in the compressed air line.
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Continuous Stirred Tank Reactor (Peristaltic Pump Feed System)

Continuous Stirred Tank Reactor (Peristaltic Pump Feed System)
 
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Product Details:
Model Name/NumberKCCRE-101B
ReactorMaterial Stainless Steel,Capacity 2 Ltrs (Approx).
StirrerStainless Steel Impeller and shaft coupled with FHP Motor
Feed TankMaterial Stainless Steel,Capacity 20 Ltrs. (Approx).
Flow MeasurementPeristaltic Pumps,2Nos. (one each for Reactants).
PipingStainless Steel and Silicon piping.

In an ideal CSTR (i.e. an ideal steady state flow reactor)the contents in reactor are well mixed and have uniformcomposition throughout. Thus the exit stream has thesame composition as the fluid within the reactor. Thistype of reactor is known as mixed flow reactor. This setupis used to study a non-catalytic homogeneous secondorder liquid phase reaction under ambient condition.The set up consists of two feed tanks through which tworeactants are fed to the reactor. Peristaltic Pumps areprovided to measure the individual flow of Chemicals.The flow rate can be adjusted by operating the valvesprovided on respective Pumps. The CSTR is fitted withstirrer for proper mixing. From top outlet of it samplesare collected for analysis.
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Continuous Stirred Tank Reactor (Constant Head Feed System)

Continuous Stirred Tank Reactor (Constant Head Feed System)
 
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Product Details:
Model Name/NumberKCCRE-101C
ReactorMaterial Stainless Steel,2Ltrs. (Approx.)
StirrerStainless Steel Impeller and shaft coupled with FHP Motor.
Feed TankMaterial Stainless Steel,Capacity - 20 Ltrs. (Approx.)
Feed CirculationBy Polypropylene magnetic pump
Flow MeasurementRotameter-2Nos. (One each for Reactants).
PipingStainless Steel and PVC/PU piping

In an ideal CSTR (i.e. an ideal steady state flow reactor)the contents in reactor are well mixed and have uniformcomposition throughout. Thus the exit stream has thesame composition as the fluid within the reactor. Thistype of reactor is known as mixed flow reactor. This setupis used to study a non-catalytic homogeneous secondorder liquid phase reaction under ambient condition.The set up consists of two over head feed tanks throughwhich two reactants are fed to the reactor. Rotametersare provided to measure the individual flow of Chemicals.The flow rate can be adjusted by operating the needlevalves provided on respective Rotameter. The CSTR isfitted with stirrer for proper mixing. From top outlet of itsamples are collected for analysis.
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Isothermal Continuous Stirred Tank Reactor

Isothermal Continuous Stirred Tank Reactor
 
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Product Details:
Model Name/NumberKCCRE-102
ReactorMaterial Stainless Steel, Capacity 2 Ltrs. (Approx.)
Water BathMaterial Stainless Steel, Double wall, insulated with Ceramic Wool
HeaterNichrome wire Heater
StirrerStainless Steel Impeller and shaft coupled with FHP Motor (One each for Water Bath and Reactor).
Feed TankMaterial Stainless Steel, Capacity-20 Ltrs. (Approx.)
Feed CirculationBy compressed air.

In an ideal CSTR (i.e. an ideal steady state flow reactor)the contents in reactor are well mixed and have uniformcomposition throughout. Thus the exit stream has thesame composition as the fluid within the reactor. Thistype of reactor is known as mixed flow reactor. This setupis used to study a non-catalytic homogeneous secondorder liquid phase reaction under isothermal condition.The set up consists of two feed tanks through which tworeactants are fed to the reactor. Rotameters are providedto measure the individual flow of Chemicals. The flowrate can be adjusted by operating the needle valvesprovided on respective Rotameter. The compressed air isused for circulation of feed. The CSTR is fitted with stirrerfor proper mixing. From top outlet of it samples arecollected for analysis. Constant temperature water batharrangement is provided to conduct the experiment atvarious temperatures. Pressure Regulator, PressureGauge and Safety Valve are fitted in the compressed airline.
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Cascade Continuous Stirred Tank Reactor

Cascade Continuous Stirred Tank Reactor
 
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Product Details:
Model Name/NumberKCCRE-103
ReactorMaterial Stainless Steel, Capacity 1 Ltr.(Approx.)
StirrerStainless Steel Impeller and shaft coupled with FHP Motor
Feed TankMaterial Stainless Steel, Capacity - 20 Ltrs. (Approx.)
Feed CirculationBy compressed air.
Flow MeasurementRotameter-2Nos. (one each for Reactants).

In an ideal CSTR (i.e. an ideal steady state flow reactor)the contents in reactor This set-up is used to study a noncatalytichomogeneous second order liquid phasereaction under ambient condition.The setup consists of three CSTR arranged in series andtwo feed tanks through which two reactants are fed tothe reactor. Rotameters are provided to measure theindividual flow of Chemicals. The flow rate can beadjusted by operating the needle valves provided onrespective Rotameter. The compressed air is used forcirculation of feed. Reactants from feed tanks enter in thefirst CSTR and are passed to second CSTR and so on. Foranalysis samples are collected from different portsprovided. Pressure Regulator, Pressure Gauge and SafetyValve are fitted in the compressed air line.
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R.T.D. Studies in Continuous Stirred Tank Reactor

R.T.D. Studies in Continuous Stirred Tank Reactor
 
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Product Details:
Model Name/NumberKCCRE-104
ReactorMaterial Stainless Steel,Capacity 2 Ltrs. (approx.)
StirrerMaterial Stainless Steel Impeller and shaft coupled with FHP motor
Feed TankMaterial Stainless Steel,Capacity - 20 Ltrs. (approx.)
Feed CirculationBy compressed air.
Flow MeasurementRotameter.
PipingStainless Steel and PU pipe

Real reactors do not satisfy the idealized flow patterns,back mix flow or plug flow deviation from ideality can bedue to channeling of fluid through the vessel, recycling offluid within the vessel or due to the presence of stagnantregion or pockets of fluid in the vessel. To predict theexact behaviour of a vessel as a Chemicals reactor, RTD orstimulus response technique is used.The setup consists of one feed tank through which wateris fed to the reactor. The flow rate can be adjusted byoperating the needle valve and measured by Rotameter.The compressed air is used for circulation of feed. Thecontinuously stirred tank reactor made of Stainless Steelis provided for understanding the R.T.D. characteristics.Pressure Regulator & Pressure Gauge are fitted in thecompressed air line.
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Plug Flow Tabular Reactor

Plug Flow Tabular Reactor
 
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Product Details:
Model Name/NumberKCCRE-105
ReactorMaterial Borosilicate Glass, OD-32mm, ID-25mm, Length-1200mm
Feed TankMaterial Stainless Steel, Capacity-20 Ltrs. (approx.)
Feed CirculationBy compressed air
Flow MeasurementRotameter-2Nos. (One each for reactants)
PipingStainless Steel and PU Pipe.
Pressure Regulator0-2 Kg/cm2

In an ideal Plug Flow Reactor (PFTR) there is no mixing inthe direction of flow and complete mixing perpendicularto direction of flow. Concentration of reactants variesalong the length of reactor but not in radial direction. Thisset-up is used to study a non-catalytic homogeneousreaction under ambient condition.The set up consists of two feed tanks through which tworeactants are fed to the reactor. Rotameters are providedto measure the individual flow of Chemicals. The flowrate can be adjusted by operating the needle valvesprovided on respective Rotameter. The compressed air isused for circulation of feed. A straight tube type reactorkept horizontally and inclined upward at outlet fromwhere samples are collected for analysis. PressureRegulator, Pressure Gauge and Safety Valve are fitted inthe compressed air line.
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Plug Flow Tubular Reactor

Plug Flow Tubular Reactor
 
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Product Details:
Model Name/NumberKCCRE-106
ReactorMaterial Stainless Steel, Volume (0.6-0.7) Ltrs (approx.).
Feed TankMaterial Stainless Steel, Capacity - 20 Ltrs. (approx.)
Feed CirculationBy compressed air.
Flow MeasurementRotameter 2Nos. (One each for Reactants).
PipingStainless Steel and PU pipe
Pressure Regulator0-2 Kg/cm2.

In an ideal Plug Flow Reactor (PFTR) there is no mixing inthe direction of flow and complete mixing perpendicularto direction of flow. Concentration of reactants variesalong the length of reactor but not in radial direction. Thisset-up is used to study a non-catalytic homogeneousreaction under ambient condition.The set up consists of two feed tanks through which tworeactants are fed to the reactor. It is a helical coil tubetype reactor. Rotameters are provided to measure theindividual flow of Chemicals. The flow rate can beadjusted by operating the needle valves provided onrespective Rotameter. The compressed air is used forcirculation of feed. Samples are collected for analysisfrom the outlet of reactor. Pressure Regulator, PressureGauge and Safety Valve are fitted in the compressed airline.
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R.T.D. Studies in Plug Flow Tubular Reactor

R.T.D. Studies in Plug Flow Tubular Reactor
 
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Product Details:
Model Name/NumberKCCRE-109
ReactorMaterial Stainless Steel,Capacity (0.6-0.7) Ltrs. (Approx.) (Helical Coiled Tube Type)
Feed TankMaterial Stainless Steel,Capacity 20Ltrs. (Approx.)
Feed CirculationBy compressed air.
Flow MeasurementBy Rotameter
PipingMaterial Stainless Steel and PU pipe
Pressure Regulator0-2 Kg/cm2

Real reactors do not satisfy the idealized flow patterns,back mix flow or plug flow deviation from ideality can bedue to channeling of fluid through the vessel, recycling offluid within the vessel or due to the presence of stagnantregion or pockets of fluid in the vessel. To predict theexact behaviour of a vessel as a Chemicals reactor, RTD orstimulus response technique is used.The setup consists of one feed tank through which wateris fed to the reactor. The flow rate can be adjusted byoperating the needle valve and measured by Rotameter.The compressed air is used for circulation of feed. It is ahelical coil tube type plug flow reactor made up ofStainless steel pipe. Reactants enter at lower end comingout of the top of coil from where samples are collectedfor analysis.For understanding the R.T.D. characteristics, a specialarrangement to inject tracer into the lower end ofreactor, using a syringe is provided. Pressure Regulator &Pressure Gauge are fitted in the compressed air line.
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Combined Flow Reactor

Combined Flow Reactor
 
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Product Details:
Model Name/NumberKCCRE-110
Reactor 1Helical Coil Tube Type, Capacity 1 Liter approx made of stainless steel 304 grade.
Reactor 2CSTR made of stainless steel 304 grade, Material Stainless Steel 304 grade, Capacity 1 Liter (approx
Stirrer for CSTRStainless Steel Impeller and shaft coupled with FHP motor
Feed TankMaterial Stainless Steel, Capacity 20 Ltrs.
Feed circulationBy compressed air
Flow MeasurementRotameter 2 Nos. (One each for Reactants).

This set-up is used to study a non-catalytic homogeneoussecond order liquid phase reaction under ambientcondition in a combined reactor. It consists of tworeactors connected in series; one is plug flow reactor andanother is CSTR.In an ideal Plug Flow Reactor (PFTR) there is no mixing inthe direction of flow and complete mixing perpendicularto direction of flow. Concentration of reactants variesalong the length of reactor but not in radial direction. Incase of a coil turbulence is introduced due to frequentchange in direction of flow and presence of secondaryflow, so a higher value of reaction rate constant isexpected in coil tube type plug flow reactor.In an ideal CSTR the contents in reactor are well mixedand have uniform composition throughout. Thus the exitstream has the same composition as the fluid within thereactor.The set up consists of two feed tanks through which tworeactants are fed to the reactors fitted in series.Rotameters are provided to measure the individual flowof Chemicals. The flow rate can be adjusted by operatingthe needle valves provided on respective rotameter. Thecompressed air is used for circulation of feed. 1st is ahelical coil tube type reactor made up of SS pipe.Reactants enter at lower end coming out of the top of coilfrom where it is fed to CSTR fitted with stirrer for propermixing. Samples are collected for analysis. PressureRegulator, Pressure Gauge and Safety Valve are fitted inthe compressed air line.
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Isothermal Batch Reactor

Isothermal Batch Reactor
 
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Product Details:
Model Name/NumberKCCRE-111
ReactorMaterial Stainless Steel, Volume 2 Ltrs. (Approx.)
Water BathMaterial Stainless Steel, Double wall, insulated with Ceramic wool.
HeaterNichrome wire Heater
StirrerStainless Steel Impeller and shaft coupled with FHP moto
Temperature SensorRTD PT-100 type

A batch reactor is a closed system with no input andoutput streams. A batch reactor can operate underconditions like Isothermal (Temperature of Reaction Massremains constant), perfectly mixed (composition ofreaction mixture is uniform throughout), and constantvolume (volume of the reaction mixture within thereactor remains constant, there is no appreciable changein the density of reaction mass). This set-up is used tostudy a non-catalytic homogeneous reaction underisothermal condition.The set up consists of a Reactor fitted in a constanttemperature water bath. One stirrer is fitted for mixingthe reactants in reactor and other is fitted in water bathto keep the uniform temperature throughout in the bath.The temperature of bath can be maintained fromambient to 90ºC with the help of Digital Temperatureindicator Cum Controller. Samples can be taken out withthe help of a sampling pipette.
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Isothermal Semi-Batch Reactor

Isothermal Semi-Batch Reactor
 
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Product Details:
Model Name/NumberKCCRE-112
ReactorMaterial Stainless Steel, Capacity 2 Ltrs. (approx).
Water BathMaterial Stainless Steel, Double wall, insulated with Ceramic Wool.
HeaterNichrome wire Heater
StirrerMaterial Stainless Steel Impeller and shaft coupled with FHP motor
Feed TankMaterial Stainless Steel, Capacity 20 Ltrs.

An isothermal semi-batch reactor is a semi-closed systemwith one input stream. It is operated under conditionslike Isothermal (Temperature of Reaction Mass remainsconstant) and perfectly mixed (composition of reactionmixture is uniform throughout). This set-up is used tostudy a non-catalytic homogeneous reaction underisothermal condition.The set up consists of a Reactor fitted in a constanttemperature water bath. Before starting the reaction thereactor is charged with measured quantity of onereactant. From a feed tank another reactant is fed to thereactor. Using a sampling pipette samples can be takenout for analysis after fixed interval. Rotameter is providedto measure the flow of Chemical. The compressed air isused for circulation of feed. One stirrer is fitted for mixingthe reactants in reactor and other is fitted in water bathto keep the uniform temperature throughout in the bath.The temperature of bath can be maintained fromambient to 70ºC with the help of Digital Temperatureindicator Cum Controller. Pressure Regulator, PressureGauge and Safety Valve are fitted in the compressed airline.
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Packed Bed Reactor

Packed Bed Reactor
 
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Product Details:
Model Name/NumberKCCRE-113
Reactor ColumnMaterial Borosilicate Glass Volume 1.2 Ltrs. (Approx)
PackingRasching Rings, Material Borosilicate Glass. Size 6-8 mm (approx
Feed TankMaterial Stainless Steel, Capacity 20 Ltrs.
Feed CirculationBy compressed air
Flow MeasurementRotameter 2Nos. (One each for Reactants).
PipingStainless Steel and PU Pipe

The setup consists of a glass column packed withRasching Rings and two feed tanks. Reactants are fed tothe reactor through liquid distributor, fitted at thebottom of the column. Rotameters are provided tomeasure the individual flow of Chemicals. The flow ratecan be adjusted by operating the needle valves providedon respective Rotameter. The compressed air is used forcirculation of feed. Samples can be taken periodicallyfrom the top outlet of reactor. Pressure Regulator &Pressure Gauge are fitted in the compressed air line.
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Hydrodynamics Of Trickle Bed Reactor

Hydrodynamics Of Trickle Bed Reactor
 
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Product Details:
Model Name/NumberKCCRE-120
Packed BedMaterial Borosilicate Glass Dia. 80mm, Height 600mm
PackingsGlass Beads Dia. 3mm/Rasching Rings, size 8-10mm
Flow measurementBy Rotameter-2Nos. (One each for water and air).
Liquid Feed TankMaterial Stainless Steel, Capacity 60 Ltrs. (Approx.)
Feed CirculationCentrifugal Pump, FHP Crompton/Standard make.

The set-up consists of a glass column. Arrangement ismade for changing the glass column conveniently andfilling it with any type of packing required. Air from aregulated pressure vessel passes through a sparger andallowed to enter in the column at the top. Liquid is feedfrom a tank, fitted with a pump and is distributed at thetop of a column using a spray nozzle. Set-up is fullyaccompanied with manometers required. Solenoid valvesare provided in the feed line at the top of column forinstant release and close. The flow rate can be adjustedby operating the valves provided in respective line.
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Annular UV Photo Reactor

Annular UV Photo Reactor
 
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Product Details:
Model Name/NumberKCCRE-121
UV Source30 W / 16 W
ReactorWith inside reflective surface. Effective volume of reactor (1-1.5) Ltrs.
Feed Tank MaterialMaterial Stainless Steel
Feed Tank CapacityCapacity 5 Ltrs. (Approx.)
Flow circulationBy Peristaltic Pump (1No.)

The set-up is used to study a photo catalytic reactionusing a UV source provided in the form of an UV tube.This set-up can be used to carry out a parameter studyunder batch/continuous flow condition. A photo catalystlike TiO2 can be used. This set-up can also be used tostudy the mineralization of liquid effluent industrialstreams & for purification of water.The set-up consists of reactor with inside reflectingsurface. An UV source surrounding glass/quartz cylinder isplaced centrally in the reactor.
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Spinning Basket Reactor

Spinning Basket Reactor
 
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Product Details:
Model Name/NumberKCCRE-123
Reactor VesselMaterial Stainless Steel Effective Volume 1000 ml.
BasketMaterial Stainless Steel, Fitted with appropriate Stainless Steel.
Drive for BasketDC Motor with Thyristor controlled DC Drive for Variable Speed.
PackingCatalyst
Feed TankMaterial Stainless Steel, Capacity 10 Ltrs.
Flow MeasurementBy Rotameter

Any catalytic liquid-liquid or liquid-gas reaction involvingthe use of a catalyst placed in basket can be studies inthis set-up. Kinetic parameter of a specific reaction can beestimated & parametric studies can be conducted. Theset-up consists of a reactor centrally having one spinningbasket derived through a variable speed motor. Themetered flow of reactant from feed tank is fed to thereactor at the bottom. The set-up can be used as batchwise of as continuous type. Sampling points are providedfor analysis. Port connection for gas inlet is provided atthe bottom of the reactor.
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Kinetics of Dissolution of Benzoic Acid

Kinetics of Dissolution of Benzoic Acid
 
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Product Details:
Model Name/NumberKCCRE-119
ChamberMaterial Stainless Steel,Capacity 1 Ltrs. (approx)
Peltilizer1" Diameter,2" Height (approx). with spanner (compatible size)
StirrerMaterial Stainless Steel Impeller and shaft coupled with FHP motor

The setup consists of a Reactor in which solid cylinder ofBenzoic Acid is placed and water is stirred by means of avariable speed mixer. Baffles are also provided. TheReactor is made of Stainless Steel. A Peltilizer is providedto make the solid cylinder of size 1" diameter and 2"height of Benzoic Acid.
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Isothermal Plug Flow Tubular Reactor

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Product Details:
Model Name/NumberKCCRE-107
ReactorMaterial Stainless Steel, Capacity (0.6-0.7) Ltrs. (approx.) (Helical Coiled Tube Type)
Water BathMaterial Stainless Steel, Double wall insulated with Ceramic Wool.
HeaterNichrome wire Heater
Stirrer Water BathMaterial SS Impeller and shaft coupled with FHP motor
Feed TankCapacity-20 Ltrs. (approx.)
Feed CirculationBy compressed air

In an ideal Plug Flow Reactor (PFTR) there is no mixing inthe direction of flow and complete mixing perpendicularto direction of flow. Concentration of reactants variesalong the length of reactor but not in radial direction. Incase of a coil turbulence is introduced due to frequentchange in direction of flow and presence of secondaryflow, so a higher value of reaction rate constant isexpected in coil tube type plug flow reactor. This set-up isused to study a non-catalytic homogeneous reactionunder isothermal condition.The set up consists of two feed tanks through which tworeactants are fed to the reactor. Rotameters are providedto measure the individual flow of Chemicals. The flowrate can be adjusted by operating the needle valvesprovided on respective Rotameter. The compressed air isused for circulation of feed. It is a helical coil tube typereactor kept in a constant temperature water bath toconduct the experiment at various temperatures.Reactants enter at lower end coming out of the top of coilfrom where samples are collected for analysis. PressureRegulator, Pressure Gauge and Safety Valve are fitted inthe compressed air line.
 
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R.T.D. In Packed Bed Reactor

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Product Details:
Model Name/NumberKCCRE-114A
Reactor ColumnMaterial Borosilicate Glass
PackingRasching Rings, Material Borosilicate Glass. Size 8-10mm (approx)
Feed TankMaterial Stainless Steel, Capacity 20 Ltrs
Feed CirculationBy compressed air.
Flow MeasurementRotameter.
PipingStainless Steel and PU pipe.

Axial diffusion and dispersion of fluid in packed beds areimportant for design and operation of separationequipment and Chemicals reactors. The tracer technique,the most widely used method for the study of axialdispersion. In stimulus response experimentation, weperturb the system using pulse input of tracer and thensee how the system reacts or responds to this stimulus.The analysis of the response gives the desiredinformation about the system.The setup consists of a glass column packed withRasching Rings and one feed tank. Water is fed to thereactor through liquid distributor, fitted at the bottom ofthe column. Rotameter is provided to measure the flowof water. The flow rate can be adjusted by operating theneedle valve provided on Rotameter. For understandingthe R.T.D. characteristics, a special arrangement to injecttracer into the lower end of reactor, using a syringe, isprovided. Samples can be taken periodically from the topoutlet of reactor. Pressure Regulator & Pressure Gaugeare fitted in the compressed air line.
 
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Continuous Stirred Tank Reactor

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Product Details:
Model Name/NumberKCCRE-116
ReactorMaterial SS, Capacity 0.5-1.5 Ltrs. (Approx.)
AgitatorVariable speed with speed control facility
ImpellerMaterial Stainless Steel, 4 Square bladed (1 No.)
Baffles4 Nos., Detachable.
Heating CoilMaterial Stainless Steel for heating purpose.

The set is mounted on the base plate and easily can beinstalled on the chemical reactor service unit forconducting experiments. Reactants are fed to the systemand mixed in the reactor. A variable speed mixer withspeed control facility is provided to conduct theexperiment on different speed of the impeller thus todetermine the effect of mixer speed. Detachable bafflesalso accompany the reactor vessel. A coil is placed in thereactor through whom hot water with constanttemperature is circulated which enables to enhance theexperimentations for different temperature.
 
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Liquid Phase Chemical Reactor

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Product Details:
Model Name/NumberKCCRE-118
ReactorMaterial SS, Capacity (1-2) Ltrs
AgitatorVariable speed with speed control facility from 0 - 150 RPM.
Impeller4 Square bladed (1 No.), Material- Stainless Steel
BafflesDetachable.
PipingPVC

Present set-up consists of a reactor vessel fitted withvariable speed agitator and detachable baffles. This unit isdesigned to study chemical kinetics. Reactants are fed tothe reactor, using pump and flow is regulated andmonitored by individual Rotameter. An adjustableoverflow device is provided in the reactor to conduct theexperiment on different reactor volume.A Stainless Steel Coil is immersed in the reactor throughwhich the hot water supply is circulated. Temperature ofthe hot water is controlled by means of TemperatureController and it enables the students to enhance theexperimentation capabilities.
 
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Recycled Bed Reactor

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Product Details:
Model Name/NumberKCCRE-122
Reactor ColumnMaterial Stainless Steel Diameter 25mm (approx.), Length 500mm (approx.).
PackingCatalyst
Feed TankMaterial Stainless Steel, Capacity 20 Ltrs.
Flow MeasurementBy Peristaltic Pump (2Nos.)
PipingStainless Steel and PVC.
Hot water tankMade of Stainless steel, Double wall, insulated with Ceramic Wool. Capacity (10-15) ltrs.

The setup consists of catalyst packed column of StainlessSteel. Reactant from a feed tank is fed to the reactorthrough liquid distributor, fitted at one end of thecolumn. Some part of product is recycled to the reactorusing peristaltic pump. Peristaltic Pumps are provided tomeasure the individual flow of feed & recycled product.The feed rate and recycle product ratio can be operatedby the respective peristaltic Pumps. Samples can be takenperiodically from the top outlet of reactor at another end.An arrangement is made to carry out the reaction atIsothermal conditions by circulating the hot water in theouter jacket of the packed bed reactor. Arrangement isdone for proper mixing is done of feed & recycle productbefore its entry to the reactor.
 
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Emulsion Polymerization Reactor

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Product Details:
Model Name/NumberKCCRE-124
Reactor Jacketed TypeMaterial Stainless Steel Total volume of Reactor 1.5-2 Ltrs. (approx.)
AgitatorMaterial Stainless Steel Impeller (2 paddles) fitted with Stainless Steel Shaft coupled to DC Motor
Flow MeasurementBy Rotameter (for Nitrogen Gas)
De Oxygenation ColumnCompatible capacity.
Hot Water TankMaterial Stainless Steel, Double Wall, insulated with ceramic wool.
Hot water circulationMagnetic Pump made of Polypropylene. Maximum working temperature is 80 degree C.

The set-up is used to carry out the emulsionpolymerization involving polymerization of a unsaturatedmonomer like Styrene. Emulsion is of the type: oil inwater, monomer is oil soluble & the initiator is watersoluble& an emulsifier is used to create a stableemulsion. Apparatus can be used to generate the kineticdata for emulsion polymerization under various operatingconditions like temperature, emulsifier concentration etc.Polymerization is carried out under the atmosphere of airfree nitrogen. The set-up consists of jacketed type SSreactor fitted with a variable speed agitator & baffles. Hotwater from a digitally controlled water bath is circulatedin the jacket using a pump. Metered quantity of nitrogengas from a cylinder passes through a de-oxygenationcolumn & allowed to enter in the reactor. Air has to beevacuated using a vacuum pump to create vacuum up to30mm of Hg before passing the nitrogen supply. Initiatorfrom reservoir is supplied to the reactor under pressure.Set-up is complete & self-contained with sampling ports.
 
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Adiabatic Batch Reactor

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Product Details:
Model Name/NumberKCCRE-117
Reactor MaterialMaterial Stainless Steel
Reactor Capacity1 Ltrs. (Approx)
Reactor Insulated withCeramic wool
StirrerTeflon Impeller and Stainless Steel shaft coupled with FHP motor

An adiabatic batch reactor is a closed system with noinput and output streams. This reactor is operated underconditions like adiabatic (Temperature of Reaction Masskeep on changing), Perfectly mixed (composition ofreaction mixture is uniform throughout), and constantvolume (volume of the reaction mixture within thereactor remains constant, there is no appreciable changein the density of reaction mass). This set-up is used tostudy a catalytic homogeneous reaction under adiabaticcondition.The set-up consists of a Dewar flask of capacity 1 lit. fittedwith a stirrer. The flask is double insulated by ceramicwool insulation. Temp. is measured by digital tempindicator. The whole setup is mounted on a rigid M.S.frame.
 
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